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Structure, properties and wear performance of nano-multilayered TiAlCrSiYN/TiAlCrN coatings during machining of Ni-based aerospace superalloys

机译:镍基航空高温合金加工过程中纳米多层TiAlCrSiYN / TiAlCrN涂层的结构,性能和耐磨性能

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New nano-multilayered TiAlCrSiYN/TiAlCrN coatings have been developed with various ratios of Ti/Al/Cr within Si. +. Y containing nano-layers.The layered nanostructure of the coatings has been studied by STEM-HAADF mode and the nano-metric composition obtained by in-situ EDS. Micro-mechanical characteristics were investigated using a Micro Materials NanoTest System. Thermogravimetric-Differential Thermal Analysis (TG-DTA) was used within a temperature range of 25-1200~°C for oxidation resistance evaluation.The wear performance of nano-multilayered TiAlCrSiYN/TiAlCrN coatings during machining of direct aged Inconel (DA) 718 and powder metallurgical ME 16 Ni-based superalloys has been investigated. The kinetic coefficient of friction under metal cutting conditions of Inconel was measured. The temperature range was 25-1000~°C.It was shown that the composition of the nano-multilayered coatings and their characteristics have to be tuned for specific applications. A nano-multilayered coating with increased amount of Al (60. at.%) in Si. +. Y containing nano-layers that has strong oxidation resistance and a higher range of micro-mechanical properties related to crack propagation under scratch conditions behaves better during machining of Inconel DA 718 alloy. For machining of the more high temperature strong and thermally resistant ME 16 superalloy, a nano-multilayered coating with less Al (55. at.%) in Si. +. Y containing nano-layers that combines improved oxidation resistance with higher hardness and other beneficial micro-mechanical properties associated with resistance to plastic deformation performs best.
机译:已经开发出具有不同比例的Si中的Ti / Al / Cr的新型纳米多层TiAlCrSiYN / TiAlCrN涂层。 +。含Y的纳米层。已通过STEM-HAADF模式研究了涂层的层状纳米结构,并通过原位EDS研究了纳米级组成。使用Micro Materials NanoTest系统研究了微机械特性。在25-1200〜°C的温度范围内使用热重差热分析(​​TG-DTA)进行抗氧化性评估。纳米多层TiAlCrSiYN / TiAlCrN涂层在直接时效Inconel(DA)718和Inconel(DA)718加工过程中的磨损性能已经研究了粉末冶金ME 16 Ni基高温合金。测量了因科镍合金在金属切削条件下的动摩擦系数。温度范围为25-1000°C,表明纳米多层涂层的组成及其特性必须针对特定应用进行调整。一种纳米多层涂层,其中Si中的Al含量增加(60 at。%)。 +。在Inconel DA 718合金的机械加工过程中,具有Y的纳米层具有强的抗氧化性,并且与在刮擦条件下的裂纹扩展相关的更高的微机械性能范围更佳。为了加工更高温度的强度高且耐热的ME 16超级合金,是一种纳米多层涂层,其中的Al含量少于Si(55at。%)。 +。结合了改进的抗氧化性和更高的硬度以及与抗塑性变形相关的其他有益的微机械性能的含Y纳米层表现最佳。

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