Expeditious microwave-assisted thionation with the system PSCl3/H2O/Et3N under solvent-free condition

Pathak U; Pandey LK; Tank R

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Expeditious microwave-assisted thionation with the system PSCl3/H2O/Et3N under solvent-free condition

机译：在无溶剂条件下使用PSCl3 / H2O / Et3N系统进行快速微波辅助硫磺化

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A novel thionation protocol for carbonyl compounds, with the system PSCl3/H2O/Et3N has been discovered. Clean, rapid, and efficient synthesis of a variety of thiocarbonyl compounds such as thioamides, thiolactams, thioketones, thioxanthones, and thioacridone can be achieved through this simple and convenient method under solventless condition with microwave irradiation.

机译：已经发现了一种新的羰基化合物硫磺化方案，系统为PSCl3 / H2O / Et3N。通过这种简单方便的方法，在无溶剂条件下用微波辐照，可以清洁，快速，有效地合成各种硫代羰基化合物，例如硫代酰胺，硫代内酰胺，硫代酮，噻吨酮和硫代rid啶酮。

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来源
《The Journal of Organic Chemistry》 |2008年第7期|共4页
作者
Pathak U; Pandey LK; Tank R;
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正文语种 eng
中图分类有机化学;
关键词
ORGANOPHOSPHORUS COMPOUNDS; LAWESSONS REAGENT; THIOAMIDES; CONVERSION; THIOKETONES; THIONES; AMIDES;

机译：有机磷化合物;洛桑试剂;硫酰胺;转化;硫酮;亚硫胺;酰胺;

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专利

1. Expeditious microwave-assisted thionation with the system PSCl3/H2O/Et3N under solvent-free condition [J] . Pathak U, Pandey LK, Tank R The Journal of Organic Chemistry . 2008,第7期

机译：在无溶剂条件下使用PSCl3 / H2O / Et3N系统进行快速微波辅助硫磺化
2. Microwave-assisted synthesis of 1,2,4- triazolo[4,3-a] [1,8]naphthyridines using FeCl3.6H2O under solvent-free conditions [J] . K Mogilaiah, R Shiva Prasad, J Kumara Swamy Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2010,第3期

机译：在无溶剂条件下使用FeCl3.6H2O微波辅助合成1,2,4-三唑并[4,3-a] [1,8]萘啶
3. Iodination of Organic Compounds Using the Reagent System I2-30% aq.H2O2 under Organic Solvent-free Reaction Conditions [J] . Jasminka Pavlinac, Marko Zupan, Stojan Stavber Acta Chimica Slovenica . 2008,第4期

机译：在无有机溶剂的反应条件下，使用试剂体系I2-30％的H2O2水溶液对有机化合物进行碘化
4. Expeditious Solvent-Free Organic Syntheses Using Microwave Irradiation [C] . Rajender S. Varma Symposium on Green Chemical Syntheses and Processes, null . -1

机译：微波辐射快速实现无溶剂有机合成
5. New developments toward the synthesis of heterocycles and applications in green chemistry. I. A simple and essentially one-pot synthesis of N-aminated heterocycles using phase transfer catalyst (Aliquat-336). II. Synthesis of pharmaceutically important pyrrole derivatives. III. Applications in green chemistry: Surfactant-mediated environmentally friendly cleavage of aromatic esters and trans-esterification under solvent-free neutral conditions . [D] . Patel, Nitinchandra. 2005

机译：杂环合成的新进展及其在绿色化学中的应用。 I.使用相转移催化剂（Aliquat-336）简单且基本上一锅合成N-胺化的杂环。二。药学上重要的吡咯衍生物的合成。三，在绿色化学中的应用：在无溶剂的中性条件下，表面活性剂介导的环境友好的芳族酯裂解和酯交换反应。
6. Microwave-Assisted Expeditious Synthesis of 2-Alkyl-2-(N-arylsulfonylindol-3-yl)-3-N-acyl-5-aryl-134-oxadiazolines Catalyzed by HgCl2 under Solvent-Free Conditions as Potential Anti-HIV-1 Agents [O] . Zhiping Che, Yuee Tian, Shengming Liu, 2018

机译：无溶剂条件下HgCl2催化微波辅助快速合成2-烷基-2-（N-芳基磺酰基吲哚-3-基）-3-N-酰基-5-芳基-134-恶二唑啉-HIV-1剂
7. Expeditious Microwave-Assisted Thionation with the System PSCl3/H2O/Et3N under Solvent-Free Condition [O] . Uma Pathak, Lokesh Kumar Pandey, Rekha Tank 2009

机译：在无溶剂条件下用系统PSCl3 / H2O / ET3N迅速微波辅助。

Expeditious microwave-assisted thionation with the system PSCl3/H2O/Et3N under solvent-free condition

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