Synthesis of cystine-rich peptides

摘要

Abbreviations used:Acm,acetamidomethyl;Boc,tert-butoxycarbonyl;Bzl,benzyl;Bzl(4-Me),4-methylbenzyl;DPDS,di(2-pyridyl)disulfide;DMSO,dimethylsulfoxide;Fmoc,9-fluorenylmethoxycarbonyl;Mob,4-methoxybenzyl;Npys,3-nitro-2-pyridylsulfanyl;Pys,2-pyridylsulfanyl;StBu,tert-butylsulfanyl;sec,selenocysteine;tBu,tert-butyl;TFA,trifluoroacetic acid;TfOH,trifluoromethanesulfonic acid;Trt,trityl;Xan,9H-xanthen-9-yl.