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Effects of SiC particles size on electrochemical properties of electroless Ni-P-SiC nanocomposite coatings

机译:SiC粒径对化学镀Ni-P-SiC纳米复合涂层电化学性能的影响

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摘要

Silicon carbide (SiC) nanoparticles were co-deposited by electroless deposition in nickel-phosphorous (Ni-P) acidic bath. In order to understand the size effect of SiC nanoparticles on the electrochemical properties of the coatings, SiC nano particles with different size (20, 50 and 200 nm) in 2 g/L concentration was added to the bath. All samples was heat treated in 400A degrees C in order to obtain crystalline structure. Potentiodynamic polarization and electrochemical impedance spectroscopy was employed to examine of corrosion performance of the coatings. X-ray diffraction (XRD) and Scanning Electron Microscopy (SEM) were used for phase and morphological studies, respectively. Experimental results show that SiC particles size in the coating bath affected both composition and morphology of the coating. Presence of SiC nanoparticles in the Ni-P coating with 50 nm increased the corrosion resistance of the coating more than the other sizes.
机译:碳化硅(SiC)纳米粒子通过化学沉积在镍-磷(Ni-P)酸性镀液中共沉积。为了了解SiC纳米颗粒对涂层电化学性能的尺寸影响,将2 g / L浓度的不同尺寸(20、50和200 nm)的SiC纳米颗粒添加到镀液中。为了获得晶体结构,将所有样品在400A℃下热处理。电位动力学极化和电化学阻抗谱用于检查涂层的腐蚀性能。 X射线衍射(XRD)和扫描电子显微镜(SEM)分别用于相和形态研究。实验结果表明,镀液中的SiC颗粒尺寸会影响镀层的组成和形态。 50 nm的Ni-P涂层中存在SiC纳米颗粒比其他尺寸的涂层增加了涂层的耐腐蚀性。

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