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Starch consolidation of M3/2 high speed steel powder - influence of process parameters on resulting microstructure

机译:M3 / 2高速钢粉的淀粉固结-工艺参数对所得组织的影响

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摘要

The possibility to produce near net shape high speed steel components with an adequate microstructure by the combination of starch consolidation (SC) and super solidus liquid phase sintering (SLPS) has been evaluated using a gas atomised M3/2 high speed steel (HSS) powder. Characterisation of the green body and as sintered microstructures using light optical microscopy (LOM), scanning electron microscopy (SEM), and energy dispersive X-ray spectroscopy (EDX) reveals that both the SC and SLPS processes strongly influence the resulting microstructure and thus the properties of the high speed steel material. The results obtained show that the morphology and distribution of starch to a high extent affect the green body surface strength and that the large pores remaining after sintering originates from entrapped air introduced in the fabrication process of the green body. The results illuminate the possibility to combine SC and SLPS to produce HSS components with fully dense microstructures and retained green body geometry from a powder with particle size distribution 50-150 μm.
机译:通过使用气体雾化的M3 / 2高速钢(HSS)粉末,已经评估了通过淀粉固结(SC)和超固相液相烧结(SLPS)的组合生产具有适当微结构的近净形高速钢组件的可能性。使用光光学显微镜(LOM),扫描电子显微镜(SEM)和能量色散X射线光谱(EDX)对生坯和烧结微结构进行表征,发现SC和SLPS过程均会强烈影响所得的微结构,因此,高速钢材料的性能。所得结果表明,淀粉的形态和分布在很大程度上影响生坯的表面强度,并且烧结后残留的大孔源自生坯制造过程中引入的残留空气。该结果阐明了将SC和SLPS结合以从颗粒尺寸分布为50-150μm的粉末生产具有完全致密的微观结构和保留生坯几何形状的HSS组件的可能性。

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