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Formation of Voids in Composite Laminates: Coupled Effect of Moisture Content and Processing Pressure

机译:复合材料层压板中空隙的形成:水分含量和加工压力的耦合效应

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Void formation as a result of prepreg moisture content and processing pressure during cure was experimentally investigated in thermosetting composite laminates. This was achieved by determining the void contents of eight-ply laminates fabricated from TenCate((R)) BT250/7781 E-glass/epoxy prepreg at processing pressures of 1.7, 3.0, 4.4, and 5.8 atm. At each processing pressure, three types of laminates were fabricated using: (i) unconditioned prepregs (direct from the storage bag); (ii) prepregs conditioned at 25% relative humidity; and (iii) 99% relative humidity. Dynamics of prepreg moisture uptake during conditioning was measured using a moisture analyzer and was shown to exhibit Fickian diffusion behavior. The void contents of the cured laminates were found to vary from 1.6% to 5.0% depending on humidity environment the prepregs were exposed and the pressure applied during fabrication. The void contents of all laminates were observed to approach an asymptotic value of approximate to 1.6% as pressure was increased. The experimental results indicated the processing pressure applied during fabrication was increasingly carried by the fiber bed, reducing resin pressure during cure. Therefore, an enhanced void formation model was proposed through the addition of a pressure reduction factor and an asymptotic void content term. The proposed model was found to accurately predict the void content of laminates made of prepregs exposed to constant/varying humidity environments and fabricated at a wide range of processing pressures. POLYM. COMPOS., 36:376-384, 2015. (c) 2014 Society of Plastics Engineers
机译:在热固性复合层压板中,通过实验研究了预浸料的水分含量和固化过程中的加工压力所导致的空隙形成。这是通过确定在1.7、3.0、4.4和5.8 atm的加工压力下由TenCate BT250 / 7781电子玻璃/环氧预浸料制成的八层层压板的空隙含量来实现的。在每种加工压力下,使用以下材料制造三种类型的层压板:(i)未经调节的预浸料(直接来自储物袋); (ii)预浸料的相对湿度为25%; (iii)99%相对湿度。使用水分分析仪测量了调理过程中预浸料吸收水分的动力学,并显示出Fickian扩散行为。发现固化层压材料的空隙含量在1.6%至5.0%之间变化,这取决于预浸料暴露的湿度环境和在制造过程中施加的压力。观察到,随着压力的增加,所有层压板的空隙含量都接近约1.6%的渐近值。实验结果表明,在制造过程中施加的加工压力越来越多地由纤维床承载,从而降低了固化过程中的树脂压力。因此,通过增加减压因子和渐近孔隙含量项,提出了一种改进的孔隙形成模型。发现所提出的模型可以准确预测由暴露于恒定/变化的湿度环境并在很宽的加工压力下制造的预浸料制成的层压板的空隙率。 POLYM。 COMPOS。,36:376-384,2015.(c)2014年塑料工程师学会

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