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Morphological, Mechanical, and Thermal Characterization of Biopolymer Composites Based on Pdlylactide and Nanographite Platelets

机译:基于Pdlylactide和纳米石墨薄片的生物聚合物复合材料的形态,机械和热表征

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摘要

This work focuses on development and optimization of polylactide (PLA) and nanographite platelets (NGP) based composites to display possible superior mechanical and improved thermal stability. Melt blending and dry mixing methods of fabrication were employed at temperature of 180 C. Different Loading fractions of NGP were incorporated into polymer matrix. Morphological evaluation techniques such as XRD and TEM were applied to determine the degree of dispersion of NGPs into PLA matrix. Mechanical properties were evaluated and correlated to structural morphologies of PLA/NGP composites. Thermal properties of composites were studied to examine possible changes in T_g, T_c, T_m, and percentage crystallinity of these composites. The effect of mixing was also explored through double extrusion of some samples. It was concluded that composites containing 3 wt% NGP showed optimum mechanical performance without any significant changes in the thermal characteristics.
机译:这项工作致力于基于聚丙交酯(PLA)和纳米石墨薄片(NGP)的复合材料的开发和优化,以显示出可能的优异机械性能和改善的热稳定性。在180°C的温度下采用熔融共混和干混的制造方法。将NGP的不同负载量掺入聚合物基质中。应用XRD和TEM等形态学评估技术确定NGP在PLA基质中的分散程度。评估机械性能并将其与PLA / NGP复合材料的结构形态相关。研究了复合材料的热性能,以检查T_g,T_c,T_m和这些复合材料的结晶度百分比的可能变化。还通过一些样品的双重挤压来探索混合的效果。结论是,含有3 wt%NGP的复合材料显示出最佳的机械性能,而热特性没有任何显着变化。

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