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NIR Reflectance Spectroscopy for Nondestructive Moisture Content Determination in Peanut Kernels

机译:NIR反射光谱法测定花生仁中的无损水分

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There are some commercial instruments available that use near-infrared (NIR) radiation measurements to determine the moisture content (MC) of a variety of grain products, such as wheat and corn, without the need of any sample grinding or preparation. However, to measure the MC of peanuts with these instruments, the peanut kernels have to be chopped into smaller pieces and filled into the measuring cell. This is cumbersome, time consuming, and destructive. An NIR reflectance method is presented here by which the average MC of about 100 g of whole kernels could be determined rapidly and nondestructively. The MC range of the peanut kernels tested was between 8% and 26%. Initially, NIR reflectance measurements were made at 1 nm intervals in the wavelength range of 1000 to 1800 nm, and the data were modeled using partial least squares regression (PLSR). The predicted values of the samples tested in the above range were compared with the values determined by the standard air-oven method. The predicted values agreed well with the air-oven values, with an R 2 value of 0.93 and a standard error of prediction (SEP) of 1.18. Using the PLSR beta coefficients, five key wavelengths were identified, and MC predictions were made using multiple linear regression (MLR). The R 2 and SEP values of the MLR model were 0.91 and 1.09, respectively. Both methods performed satisfactorily and, being rapid, nondestructive, and noncontact, may be suitable for continuous monitoring of MC of grain and peanuts as they move on conveyor belts during their processing
机译:有一些商用仪器可以使用近红外(NIR)辐射测量来确定各种谷物产品(例如小麦和玉米)的水分含量(MC),而无需进行任何样品研磨或制备。但是,要使用这些仪器测量花生的MC,必须将花生仁切成小块,然后装入测量室中。这麻烦,费时且具有破坏性。本文介绍了一种近红外反射方法,通过该方法可以快速,无损地确定约100 g整个籽粒的平均MC。测试的花生仁的MC范围在8%至26%之间。最初,在1000至1800 nm的波长范围内以1 nm的间隔进行NIR反射率测量,并使用偏最小二乘回归(PLSR)对数据进行建模。将在上述范围内测试的样品的预测值与通过标准烤箱法确定的值进行比较。预测值与烤箱数值非常吻合,R 2 值为0.93,预测标准误差(SEP)为1.18。使用PLSR beta系数,确定了五个关键波长,并使用多元线性回归(MLR)进行了MC预测。 MLR模型的R 2 和SEP值分别为0.91和1.09。两种方法均令人满意地执行,并且快速,无损且无接触,可能适合连续监测谷物和花生在加工过程中在传送带上移动时的MC

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