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Study of microcapillary pipette-assisted method to prepare polyethylene glycol-coated microcantilever sensors

机译:微毛细管移液器辅助制备聚乙二醇涂层微悬臂梁传感器的研究

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摘要

Microcantilever sensors were prepared by direct deposition of polyethylene glycol (PEG) onto the microcantilever surfaces using a micro-capillary pipette. The physical properties of the PEG coatings: mass, surface area, volume and thickness were studied. The sensors were tested by exposing them to trace ethanol vapor and the physical properties of the micropipette-deposited PEG coatings were correlated with sensor response. Most of the PEG-coated microcantilevers demonstrated reproducible bending signals upon repeated exposure to ethanol (EtOH) vapor. Evident in the study is that uniformity in the gross morphology and surface structure of the PEG coating was not required for good sensor response. However, the location of the PEG on the microcantilever, PEG film thickness and surface area contributed to optimum response to exposure to EtOH vapor. The results demonstrate the utility of direct application of coatings onto microcantilevers by the micropipette technique. This method of coating microcantilevers is particularly appealing when quick, repeated tests of coated microcantilever sensors are desired as an alternative to more complex and time-consuming coating techniques.
机译:通过使用微毛细管移液管将聚乙二醇(PEG)直接沉积到微悬臂梁表面上来制备微悬臂梁传感器。研究了PEG涂层的物理性质:质量,表面积,体积和厚度。通过将传感器暴露于痕量乙醇蒸汽中来测试传感器,并将微量移液管沉积的PEG涂层的物理性质与传感器响应相关联。重复暴露于乙醇(EtOH)蒸汽后,大多数PEG涂覆的微悬臂梁均显示出可再现的弯曲信号。研究表明,良好的传感器响应不需要PEG涂层的总体形态和表面结构均匀。但是,PEG在微悬臂梁上的位置,PEG膜的厚度和表面积有助于对暴露于EtOH蒸气的最佳响应。结果证明了通过微量移液器技术将涂层直接施加到微悬臂梁上的实用性。当需要对涂覆的微悬臂梁传感器进行快速,重复的测试以替代更复杂且耗时的涂覆技术时,这种涂覆微悬臂梁的方法特别有吸引力。

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