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Application of Graphene-Based Nanocomposites in Electrochemical Detection of Heavy Metal Ions

机译:石墨烯基纳米复合材料在重金属离子电化学检测中的应用

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摘要

The purpose of this study was to explore the application of graphene-based nanocomposites in electrochemical detection of heavy metal ions. In this study, Graphene oxide (GO) was synthesized with improved Hummers method, and flower-like MoS2/rGO nanocomposite was synthesized with hydrothermal method and used as electrode modification material. In addition, scanning electron microscopy (SEM) and X-ray images were used to observe the characterization of the prepared samples and to detect the sensitivity of four heavy metal ions under optimal experimental conditions. The results showed that the reduced graphene oxides were coated with a large number of flower-like MoS2 and laid on the reduced graphene oxides. And in electrochemical experiments, adsorption experiments and interference tests, MoS2/rGO nanocomposites showed satisfactory performance for Pb(II). Therefore, this study provided a new strategy for the development of new nanocomposites composites as electrochemical sensors to detect the heavy metal ions in the aquatic environment.
机译:这项研究的目的是探索石墨烯基纳米复合材料在重金属离子电化学检测中的应用。本研究采用改进的Hummers方法合成了氧化石墨烯(GO),并利用水热法合成了花状MoS2 / rGO纳米复合材料,并将其用作电极改性材料。此外,在最佳实验条件下,使用扫描电子显微镜(SEM)和X射线图像观察所制备样品的特征并检测四种重金属离子的灵敏度。结果表明,还原的氧化石墨烯被大量的花状MoS 2包覆并沉积在还原的氧化石墨烯上。在电化学实验,吸附实验和干扰实验中,MoS2 / rGO纳米复合材料对Pb(II)的性能令人满意。因此,本研究为开发新型纳米复合材料作为电化学传感器以检测水生环境中的重金属离子提供了新的策略。

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