Turnbuckle diamond anvil cell for high-pressure measurements in a superconducting quantum interference device magnetometer

摘要

We have developed a miniature diamond anvil cell for magnetization measurements in a widely used magnetic property measurement system commercial magnetometer built around a superconducting quantum interference device. The design of the pressure cell is based on the turnbuckle principle in which force can be created and maintained by rotating the body of the device while restricting the counterthreaded end-nuts to translational movement. The load on the opposed diamond anvils and the sample between them is generated using a hydraulic press. The load is then locked by rotating the body of the cell with respect to the end-nuts. The dimensions of the pressure cell have been optimized by use of finite element analysis. The cell is approximately a cylinder 7 mm long and 7 mm in diameter and weighs only 1.5 g. Due to its small size the cell thermalizes rapidly. It is capable of achieving pressures in excess of 10 GPa while allowing measurements to be performed with the maximum sensitivity of the magnetometer. The performance of the pressure cell is illustrated by a high pressure magnetic study of Mn3[Cr(CN)6]2⋅xH2O Prussian blue analog up to 10.3 GPa. © 2010 American Institute of Physics Article Outline INTRODUCTION EXISTING OPPOSED-ANVIL PRESSURE CELLS FOR MPMS MAGNETOMETERS DESIGN AND OPERATION TESTS AND RESULTS MAGNETIC PROPERTIES OF A PRUSSIAN BLUE ANALOG UNDER PRESSURE CONCLUSIONS