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Accelerated weathering of bolted joints prepared from woven glass fiber-reinforced nanocomposites

机译:玻璃纤维增​​强纳米复合材料制备的螺栓连接的加速风化

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This work deals with the accelerated aging of the bolted joints prepared from glass fiber-reinforced nanocomposite laminates. ASTM D5961 was used to design the bolted joint, and the geometric parameters, i.e. width-to hole-diameter (W/D) ratio and edge distance-to-hole diameter (E/D) ratio were fixed to 6 and 5, respectively. ASTM D1544 was used for accelerated aging, and a maximum of 500 h cyclical ultraviolet exposure, 8 h of ultraviolet radiation at 60 celcius followed by 4 h of condensation at 50 celcius, was given to the specimens. A full factorial design of experiment was conducted on important control factors, i.e. aging time, bolt torque, and material variation, using response surface methodology. To investigate the effect of nanoclay content, a range of 0-5 wt% was investigated. Specimens with 3 wt% of nanoclay demonstrated optimum tensile strength and were selected to manufacture the bolted joint. Nanoplatelets having high aspect ratio increased the specific surface area and thus the tensile strength of the nanocomposite. It was found that the strength of the joints prepared with and without the nanoclay content decreased with the increase in the duration of aging. However, the joints with the nanoclay content had higher failure loads. The strength retention in the joints with nanoclay content was more in comparison to the joints made with neat epoxy. Nanoclay acted as a mechanical interlock at the fiber-matrix interface and improved the interfacial bond strength. A good dispersion of nanoclay also acts as a barrier to the moisture, which eventually reduces the degradation of the composite material due to the lesser fiber-matrix de-bonding under accelerated aging conditions.
机译:这项工作涉及由玻璃纤维增​​强的纳米复合材料层压板制备的螺栓连接的加速老化。使用ASTM D5961设计螺栓连接,并将几何参数(即宽径比(W / D)和边距外径(E / D))分别固定为6和5。 。使用ASTM D1544加速老化,并向样品提供最长500小时的循环紫外线照射,60摄氏度的紫外线辐射8个小时,然后在50摄氏度的冷凝4小时。使用响应曲面方法对重要的控制因素(即老化时间,螺栓扭矩和材料变化)进行了全面的因子设计实验。为了研究纳米粘土含量的影响,研究了0-5wt%的范围。具有3 wt%纳米粘土的样品显示出最佳的拉伸强度,并被选择用于制造螺栓连接。具有高纵横比的纳米片增加了比表面积,并因此增加了纳米复合材料的拉伸强度。发现随着老化时间的增加,具有和不具有纳米粘土含量的情况下制备的接头的强度降低。然而,具有纳米粘土含量的接头具有较高的破坏载荷。与用纯环氧树脂制成的接头相比,具有纳米粘土含量的接头的强度保持率更高。纳米粘土在纤维-基质界面处起机械联锁作用,并提高了界面粘结强度。纳米粘土的良好分散性也可作为水分的屏障,由于加速老化条件下纤维-基体的脱粘性较小,最终减少了复合材料的降解。

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