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Effect of alkali treatment on properties of unidirectional isora fibre reinforced epoxy composites

机译:碱处理对单向等离子纤维增强环氧复合材料性能的影响

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Unidirectional isora fibre reinforced epoxy composites were prepared by compression moulding. Isora is a natural bast fibre separated from Helicteres isora plant by retting process. The effect of alkali treatment on the properties of the fibre was studied by scanning electron microscopy (SEM), IR, thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC). Mechanical properties such as tensile strength, Young's modulus, flexural strength, flexural modulus and impact strength of the composites containing untreated and alkali treated fibres have been studied as a function of fibre loading. The optimum fibre loading for tensile properties of the untreated fibre composite was found to be 49% by volume and for flexural properties the loading was optimised at ∼45%. Impact strength of the composite increased with increase in fibre loading and remained constant at a fibre loading of 54·5%. Alkali treated fibre composite showed improved thermal and mechanical properties compared to untreated fibre composite. From dynamic mechanical analysis (DMA) studies it was observed that the alkali treated fibre composites have higher E' and low tan δ maximum values compared to untreated fibre composites. From swelling studies in methyl ethyl ketone it was observed that the mole percentage of uptake of the solvent by the treated fibre composites is less than that by the untreated fibre composites. From these results it can be concluded that in composites containing alkalised fibres there is enhanced interfacial adhesion between the fibre and the matrix leading to better properties, compared to untreated fibre composites.
机译:通过压缩模塑法制备了单向的艾索拉纤维增强环氧复合材料。 Isora是通过解胶工艺从Helicteres isora植物中分离出的天然韧皮纤维。通过扫描电子显微镜(SEM),红外光谱,热重分析(TGA)和差示扫描量热法(DSC)研究了碱处理对纤维性能的影响。已经研究了包含未经处理和经碱处理的纤维的复合材料的机械性能,例如拉伸强度,杨氏模量,弯曲强度,弯曲模量和冲击强度,与纤维负载的关系。发现未处理的纤维复合材料的拉伸性能的最佳纤维负载量为49%(体积),而挠曲性能的最佳负载量约为45%。复合材料的冲击强度随着纤维载荷的增加而增加,并且在纤维载荷为54·5%时保持恒定。与未处理的纤维复合材料相比,碱处理的纤维复合材料显示出改善的热性能和机械性能。从动态力学分析(DMA)研究发现,与未处理的纤维复合材料相比,碱处理的纤维复合材料具有较高的E'和较低的tanδ最大值。从对甲乙酮的溶胀研究中可以看出,处理过的纤维复合材料吸收溶剂的摩尔百分数小于未处理过的纤维复合材料吸收溶剂的摩尔百分数。从这些结果可以得出结论,与未处理的纤维复合材料相比,在包含碱化纤维的复合材料中,纤维与基质之间的界面粘合性增强,从而导致更好的性能。

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