Pd(OAc)_2-catalysed regioselective alkoxylation of aryl (β-carbolin-1-yl)methanones via β-carboline directed ortho-C(sp~2)-H activation of an aryl ring

Shivalinga Kolle; Sanjay Batra

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Pd(OAc)_2-catalysed regioselective alkoxylation of aryl (β-carbolin-1-yl)methanones via β-carboline directed ortho-C(sp~2)-H activation of an aryl ring

机译：Pd（OAc）_2催化的β-咔啉定向的邻位C（sp〜2）-H芳基环活化活化芳基（β-carbolin-1-基）甲烷的区域选择性烷氧基化

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Synthesis of (2-alkoxyphenyl)(9H-pyrido[3,4-b]indol-1-yl)methanone via Pd(OAc)_2-catalyzed regioselective alkoxylation of aryl (β-carbolin-1-yl) methanones employing p-carboline directed ortho-C(sp~2)-H activation of an aryl ring under oxidative conditions is described.

机译：Pd（OAc）_2催化的对位芳基（β-carbolin-1-yl）甲酮的区域选择性烷氧基化反应合成（2-烷氧基苯基）（9H-吡啶[3,4-b]吲哚-1-基）甲酮描述了在氧化条件下碳环芳基环的邻位-C（sp〜2）-H活化。

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《Organic & biomolecular chemistry 》 |2015年第41期| 10376-10385| 共10页
作者
Shivalinga Kolle; Sanjay Batra;
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作者单位

Medicinal and Process Chemistry Division, CSIR-Central Drug Research Institute, Sector 10, Jankipuram Extension, Sitapur Road, Lucknow-226031, UP, India;

Medicinal and Process Chemistry Division, CSIR-Central Drug Research Institute, Sector 10, Jankipuram Extension, Sitapur Road, Lucknow-226031, UP, India,Academy for Scientific and Innovative Research, New Delhi-110025, India;

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专利

1. β-Carboline-directed decarboxylative acylation of ortho-C(sp2)–H of the aryl ring of aryl(β-carbolin-1-yl)methanones with α-ketoacids under palladium catalysis [J] . Shivalinga Kolle, Sanjay Batra RSC Advances . 2016 ,第56期

机译：β-咔啉 - 甲基（β-胶蛋白-1-基）甲基酮的芳基（β-胶蛋白-1-基）甲基酮的芳基环芳环芳基环羧酸甲苯的甲羧酸酰基化，α-酮酸在钯催化下
2. beta-Carboline-directed decarboxylative acylation of ortho-C(sp(2))-H of the aryl ring of aryl(beta-carbolin-1-yl)methanones with alpha-ketoacids under palladium catalysis [J] . Kolle Shivalinga, Batra Sanjay RSC Advances . 2016 ,第56期

机译：β-咔啉 - 芳基（β-碳-1-基-1-基）甲基酮的芳基（Sp（2）） - H的甲醇环的甲醇环与钯催化下的甲酮（2）） - H指导脱羧酰化酰化
3. Pd(OAc)2?Catalyzed Alkoxylation of Arylnitriles via sp2 C?H Bond Activation Using Cyano as the Directing Group [J] . Wu Li† and Peipei Sun, †, ‡, The Journal of Organic Chemistry . 2012 ,第18期

机译：Pd（OAc）2？以氰基为指导基团通过sp2 C？H键活化催化芳腈的烷氧基化反应
4. Part I: Asymmetric synthesis of alpha-allyl-alpha-aryl alpha-amino acids. Part II: Asymmetric spirocyclization of allenyl ketones. Part III: Chemoselective activation of C(sp3)--H bond over C(sp 2)--H bond with Pd(II). [D] . Curto, John M. 2014

机译：第一部分：α-烯丙基-α-芳基α-氨基酸的不对称合成。第二部分：烯基酮的不对称螺环化。第三部分：与Pd（II）相比，C（sp3）-H键的化学选择性活化。
5. Novel Approach to Multifunctionalized Homoallylic Alcohols via Regioselective Ring Opening of Aryl Oxiranes with 3-Iodo Allenoates [O] . Adiseshu Kattuboina, Parminder Kaur, Cody Timmons, -1

机译：通过芳基氧杂环戊烷与3-碘代烯酸酯的区域选择性开环的新型方法来合成多功能的烯丙基醇
6. Aryl-Aryl Coupling Reaction Using a Novel and Highly Active Palladium Reagent Prepared from Pd(OAc)2, 1,3-Bisdiphenylphosphinopropane (DPPP), and Bu3P. [O] . Takashi Harayama, Toshihiko Akiyama, Yuichiro Nakano, 2002

机译：芳基芳基偶联反应使用由Pd（OAc）2,1,3-双烷基膦基的Pd（OAC）2,1,3-双烷基膦基的丙烷（DPPP）和BU3P制备的新型和高活性钯试剂。

Pd(OAc)_2-catalysed regioselective alkoxylation of aryl (β-carbolin-1-yl)methanones via β-carboline directed ortho-C(sp~2)-H activation of an aryl ring

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