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Fabrication of conductive human bio-nanoelectrode from graphene oxide modified with polyvinyl alcohol

机译:用聚乙烯醇改性的氧化石墨烯制备导电的人体生物纳米电极

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摘要

It is time for electrodes prepared from graphene oxide (GO) to replace the traditional electrodes. However, GO is an electrically insulating material. However, in this study, a conductive electrode was prepared from GO modification with glycerol (GL) under the esterification reaction at 90 degrees C for 3 h with sulphuric acid as a catalyst under vacuum conditions. Polyvinyl alcohol (PVA) acts as a polymer host. It was mixed with GO and modification was carried out under heating conditions. The mixture of the GO/GL/PVA nanocomposite was rapidly cooled and poured into the electrode mould. Finally, it is placed in a desiccator at room temperature for two days. The characterisation (Fourier transform infrared spectroscopy, X-ray diffraction, and scanning electron microscopy) proved that the ester bond was formed and a complete distribution of GO/GL into the matrix of PVA was verified. The GO/GL/PVA nanocomposite was tested for electrocardiogram (ECG) electrodes. The biopic instrument was used to compare the behaviour of the GO/GUPVA plastic electrode and the commercial one. The results indicated that the GO/GL/PVA plastic electrode efficiently detected ECG signals after two months with high conductivity and lower noise than the commercial electrode. The GO/GL/PVA plastic electrode has been reported for the first time in the literature.
机译:现在是时候用氧化石墨烯(GO)制成的电极代替传统的电极了。但是,GO是电绝缘材料。然而,在这项研究中,导电电极是由甘油(GL)进行的GO修饰,在90°C的酯化反应下,在真空条件下,以硫酸为催化剂,制备3小时的导电电极。聚乙烯醇(PVA)充当聚合物主体。将其与GO混合并在加热条件下进行改性。将GO / GL / PVA纳米复合材料的混合物快速冷却并倒入电极模具中。最后,将其在室温下放置在干燥器中两天。表征(傅里叶变换红外光谱,X射线衍射和扫描电子显微镜)证明形成了酯键,并验证了GO / GL在PVA基质中的完全分布。对GO / GL / PVA纳米复合材料的心电图(ECG)电极进行了测试。使用biopic仪器比较GO / GUPVA塑料电极和商用电极的性能。结果表明,GO / GL / PVA塑料电极在两个月后可以有效检测到ECG信号,具有比市售电极更高的电导率和更低的噪音。文献首次报道了GO / GL / PVA塑料电极。

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  • 来源
    《Nanobiotechnology, IET》 |2019年第1期|1-5|共5页
  • 作者单位

    Menia Univ, Fac Engn, Dept Chem Engn, El Minya, Egypt;

    Menia Univ, Fac Engn, Dept Biomed Engn, El Minya, Egypt;

    Menia Univ, Fac Engn, Dept Chem Engn, El Minya, Egypt|Collage Appl Sci, Dept Engn, Sohar, Oman;

    Menia Univ, Fac Engn, Dept Chem Engn, El Minya, Egypt|Zewail City Sci & Technol, Environm Engn, Giza, Egypt;

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