Precipitation Behavior and Microstructure Evolution of Mg-Zn-Zr-Er Alloy Processed by Secondary Deformation and Heat Treatment

摘要

Preheated at 673K for 3h and 6h respectively, as-extruded Mg-9Zn-0.6Zr-2Er (wt.%) slabs with starting thickness of 8mm were hot-rolled at 673K to 2mm. The hot-rolled alloys were then solution treated at 673K for 1.5h and aged at 473K for 10h. Microstructure evolution and second phase precipitation behavior during hot rolling and subsequent heat treatments were examined by optical microscopy (OM), scan electron microscopy (SEM) and micro hardness test. Mg-9Zn-0.6Zr-2Er alloy were fully recrystallized with fine equiaxed grains after preheating for 3 hours, prolonging heating time leads to a higher degree of dissolution of secondary phase into Mg matrix but a coarsening of the microstructure. During hot rolling process, the volume fraction of the DRX grains increased gradually with increasing reduction ratio, shearing bands became visble in the final pass. Thermal stable Mg-Zn-Er intermetallic compounds distributed along rolling direction at the first rolling passes and became more homogenous in the final pass. More nano-sized MgZn_2 precipitated during hot rolling in the alloy preheated for 6h than that for 3h, leading to an enhanced precipitation hardening effect in the former.