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Effect of Precipitates on Austenite Grain Growth Behavior in a Low-Carbon Nb-V Microalloyed Steel

机译:沉淀物对低碳Nb-V微合金钢中奥氏体晶粒长大行为的影响

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The effect of precipitates on austenite grain growth behavior in a Nb-V microalloyed steel was investigated. The precipitates were identified by selected area electron diffraction(SAED) and energy dispersive spectrometer(EDS) analysis. Because of pinning effect of NbC and/or VC on austenite grain boundaries, grains grew slowly at 850℃-1000℃. However, when temperature reached 1050 ℃, abnormal grain growth was observed, which was attributed to dissolution of NbC particles. The NbC precipitates dissolved significantly at 1150 ℃. However, grain sizes were still very small. Thus, austenite grains grew rapidly at 1050-1150 ℃. The fully dissolution temperature of this steel was 1150-1250℃. Finally, the relationship between grain coarsening temperature(T_(GC)) and fully dissolution temperature(T_(DISS)) could be illustrated as follows: 100 ℃≤T_(DISS) -T_(GC)≤200 ℃. When heating temperatures were 850-1050 ℃ and 1050-1250 ℃, grain growth activation energies (0 were 59945 J/mol and 135813 J/mol, respectively. The different grain growth models were mainly caused by the gradual dissolution of NbC particles.
机译:研究了析出物对Nb-V微合金钢中奥氏体晶粒长大行为的影响。通过选择区域电子衍射(SAED)和能量色散光谱仪(EDS)分析鉴定沉淀。由于NbC和/或VC对奥氏体晶界的钉扎作用,晶粒在850℃-1000℃生长缓慢。然而,当温度达到1050℃时,观察到异常的晶粒长大,这归因于NbC颗粒的溶解。 NbC沉淀在1150℃时明显溶解。但是,晶粒尺寸仍然很小。因此,奥氏体晶粒在1050-1150℃时迅速生长。该钢的完全溶解温度为1150-1250℃。最后,晶粒粗化温度(T_(GC))和完全溶解温度(T_(DISS))之间的关系可以表示为:100℃≤T_(DISS)-T_(GC)≤200℃。当加热温度为850-1050℃和1050-1250℃时,晶粒生长活化能(0分别为59945 J / mol和135813 J / mol),不同的晶粒生长模型主要是由NbC颗粒的逐渐溶解引起的。

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