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High performance liquid chromatography analysis of monomers from one composite resin cured with different polymerisation methods

机译:用一种不同聚合方法固化的一种复合树脂中的单体的高效液相色谱分析

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Light curing based resins are extensively used in modern dentistry because they offer advantages, such as the ability to bond to the tooth structure and improved aesthetic characteristics. After polymerisation, there is a significant amount of organic compound residue unbound in the cured material. Post-cure heating of composite resin materials has recently become a popular restorative technique. With indirect composite polymerisation systems, an important perspective is the possibility of using post-polymerisation mechanisms associated with heat, pressure or high light intensity. The aim of this study is to evaluate the in vitro elution of monomers (Bis-GMA, TEGDMA, UDMA, Bis-DMA and Bis-EMA) from one composite resin during two different time periods after different polymerisation methods with high performance liquid chromatography. In the current study, the polymerisation methods affected the monomer release. The Inlay System exhibited the lowest monomer release. Post-cure heat application in autoclave after polymerisation increased the amount of released monomers.
机译:基于光固化的树脂由于具有优势,例如与牙齿结构的粘合能力和改善的美学特性,因此被广泛用于现代牙科。聚合后,固化材料中有大量未结合的有机化合物残留物。复合树脂材料的后固化加热最近已成为一种流行的修复技术。对于间接复合聚合系统,重要的观点是使用与热,压力或高光强度相关的后聚合机制的可能性。这项研究的目的是评估采用高效液相色谱法在不同聚合方法之后的两个不同时间段内,从一种复合树脂中体外洗脱单体(Bis-GMA,TEGDMA,UDMA,Bis-DMA和Bis-EMA)的能力。在当前的研究中,聚合方法影响单体的释放。嵌体系统展现出最低的单体释放。聚合后在高压釜中进行后固化加热可增加释放单体的量。

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