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Synthesis and optimization of the magnetic properties of aligned strontium ferrite nanowires

机译:取向锶铁氧体纳米线的磁性合成与优化

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High aspect ratio strontium hexaferrite nanowires were fabricated by dip coating in alumina template. Fe/Sr ratio was changed from 10 to 12 in precursor, and the samples were annealed at a range of temperatures 500-900 degrees C in order to optimize the magnetic properties of strontium ferrite in the form of nanowires. Field emission scanning electron microscope (FESEM) proved the formation of nanowires in the templates, while TEM images revealed a high degree of crystallinity. The ferrites were further characterized by X-ray diffraction (XRD) and energy dispersive X-ray spectrometer (EDS). Magnetic properties of the specimens were studied by a SQUID at 10-300 K. The results showed that the coercivity of packed density nanowires in the template was much less than that of the nanopowders. On the other hand, the coercivity of nanowires at ambient temperature was less than low temperature coercivity. (C) 2015 Elsevier Ltd. All rights reserved.
机译:通过在氧化铝模板中浸涂制备高长径比的六方锶酸锶纳米线。 Fe / Sr比从前体的10变为12,并在500-900摄氏度的温度范围内对样品进行退火,以优化纳米线形式的锶铁氧体的磁性能。场发射扫描电子显微镜(FESEM)证明了模板中形成了纳米线,而TEM图像显示出很高的结晶度。通过X射线衍射(XRD)和能量色散X射线光谱仪(EDS)进一步表征了铁氧体。通过SQUID在10-300 K下研究了样品的磁性能。结果表明,模板中堆积密度纳米线的矫顽力远小于纳米粉末。另一方面,纳米线在环境温度下的矫顽力小于低温矫顽力。 (C)2015 Elsevier Ltd.保留所有权利。

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