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Boehmite nanopetals self assembled to form rosette-like nanostructures

机译:勃姆石纳米花瓣自组装形成玫瑰花状纳米结构

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Rosette-like boehmite nanostructures were prepared successfully via a simple hydrothermal process. The obtained material was characterized with X-ray powder diffractometry (XRD), transmission electron microscopy (TEM) and scanning electron microscopy (SEM). Using Scherrer formula, the average crystallite size of the obtained boehmite rosettes was measured to be about 8 nm. It was shown that boehmite nanopetals with average width of about 41 nm determined by TEM, were formed during the hydrothermal process and then self assembled due to weak hydrogen bonds to fabricate boehmite rosettes. The specific surface area of the obtained rosette-like nanostructures was calculated through BET N_2-adsorption technique to be about 143.08 m~2/g.
机译:通过简单的水热工艺成功制备了玫瑰花状勃姆石纳米结构。通过X射线粉末衍射法(XRD),透射电子显微镜(TEM)和扫描电子显微镜(SEM)对获得的材料进行表征。使用Scherrer公式,获得的勃姆石玫瑰花结的平均微晶尺寸被测量为约8nm。结果表明,在水热过程中形成了由TEM确定的平均宽度约为41 nm的勃姆石纳米花瓣,然后由于弱的氢键而自组装成勃姆石花环。通过BET N_2吸附技术计算出所得玫瑰花状纳米结构的比表面积约为143.08 m〜2 / g。

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