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A new strategy for the preparation of porous zinc ferrite nanorods with subsequently light-driven photocatalytic activity

机译:制备具有随后光驱动的光催化活性的多孔铁氧体锌纳米棒的新策略

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摘要

Porous zinc ferrite (ZnFe_2O_4) nanorods have been synthesized by the thermal decomposition of ZnFe_2(C_2O_4)_3 nanorods precursor, which was prepared by template-, surfactant-free solvothermal method. The morphology and structure of the obtained ZnFe_2(C_2O_4)_3 nanorods precursor and porous ZnFe_2O_4 nanorods were characterized by X-ray powder diffraction, transmission electron microscopy, field emission scanning electron microscopy and high-resolution transmission electron microscopy. The results indicated that the as-synthesized ZnFe_2O_4 retained the precursor morphology of ID nanorods with diameters of 100-200 nm and lengths of several micrometers and plenty of nanoparticles were interconnected to each other to form porous nanorods. The as-prepared ZnFe_2O_4 nanorods as a kind of subsequently light-driven photocatalyst exhibited good photocatalytic decomposition activity for methylene blue (MB).
机译:通过无模板,无表面活性剂溶剂热法制备的ZnFe_2(C_2O_4)_3纳米棒前体的热分解,合成了多孔的铁酸锌(ZnFe_2O_4)纳米棒。用X射线粉末衍射,透射电子显微镜,场发射扫描电子显微镜和高分辨率透射电子显微镜对所得的ZnFe_2(C_2O_4)_3纳米棒前驱体和多孔ZnFe_2O_4纳米棒的形貌和结构进行了表征。结果表明,合成后的ZnFe_2O_4保留了直径为100-200 nm,长度为几微米的ID纳米棒的前体形态,大量的纳米粒子相互连接形成多孔纳米棒。制备的ZnFe_2O_4纳米棒作为随后的光驱动光催化剂,对亚甲基蓝(MB)具有良好的光催化分解活性。

著录项

  • 来源
    《Materials Letters》 |2011年第20期|p.3116-3119|共4页
  • 作者单位

    School of Chemistry and Chemical Engineering, Anhui University of technology, No. 59 Hudong Road, Ma'anshan 243002, Anhui Province, PR China;

    School of Chemistry and Chemical Engineering, Anhui University of technology, No. 59 Hudong Road, Ma'anshan 243002, Anhui Province, PR China;

    School of Chemistry and Chemical Engineering, Anhui University of technology, No. 59 Hudong Road, Ma'anshan 243002, Anhui Province, PR China;

    School of Chemistry and Chemical Engineering, Anhui University of technology, No. 59 Hudong Road, Ma'anshan 243002, Anhui Province, PR China;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    nanocrystalline materials; porous materials; powder technology; precursor; catalysis;

    机译:纳米晶材料;多孔材料;粉末技术;前体;催化;

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