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The preparation of iron (Ⅲ) oxide nanoparticles using W/O microemulsion

机译:W / O微乳液制备三氧化二铁纳米粒子

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摘要

Iron (Ⅲ) oxide, Fe_2O_3, nanoparticles were prepared using W/O microemulsion as the reactor. W/O microemulsion was formed using n-heptane as oil phase, water and AOT as the surfactant under the specific composition. Iron (Ⅲ) Chloride was used as a starting material and Ammonium hydroxide was a precipitating agent. Fe_2O_3, nanoparticles were then produced in situ the water core. Size of particles could be adjusted by the water content of the mixtures. The higher the water content, the bigger the particle size. The average size of the nanoparticles obtained was smaller than 100 nm. Moreover, Fe_2O_3 produced by this method was hematite with hexagonal in structure.
机译:以W / O微乳液为反应器,制备了三氧化二铁Fe_2O_3纳米粒子。在特定组成下,使用正庚烷作为油相,水和AOT作为表面活性剂形成W / O微乳液。以氯化铁(Ⅲ)为起始原料,氢氧化铵为沉淀剂。然后在水核中原位生成Fe_2O_3纳米颗粒。颗粒的大小可以通过混合物的水含量来调节。含水量越高,粒径越大。获得的纳米颗粒的平均尺寸小于100nm。另外,通过该方法制造的Fe_2O_3为具有六方晶结构的赤铁矿。

著录项

  • 来源
    《Materials Letters》 |2011年第18期|p.2820-2822|共3页
  • 作者单位

    Department of Chemistry, Faculty of Science, Rangsit University, Thailand;

    Department of Chemistry, Faculty of Science, Rangsit University, Thailand;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    w/o microemulsion; hematite; nanoparticle; fe_2o_3;

    机译:不含微乳液;赤铁矿;纳米颗粒;fe_2o_3;

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