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Optical and surface morphological properties of triethylamine passivated lead sulphide nanoparticles

机译:三乙胺钝化硫化铅纳米粒子的光学和表面形态学性质

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摘要

The triethylamine capped lead sulphide (PbS) nanoparticles were successfully synthesized by simple wet chemical method. The synthesized product has been characterized by powder X-ray diffraction (XRD), UV-vis spectrophotometry, FT1R spectroscopy, atomic force microscopy (AFM), transmission electron microscopy (TEM) and photoluminescence studies. The size of the PbS nanoparticles was determined from AFM, TEM, XRD and from these studies it is found that the size of the particles of the order of 10-15 nm. Significant "blue shift" from bulk material was observed on the PbS nanoparticles using UV-vis and photoluminescence spectrum.
机译:通过简单的湿化学方法成功地合成了三乙胺封端的硫化铅(PbS)纳米颗粒。合成的产物已通过粉末X射线衍射(XRD),紫外可见分光光度法,FT1R光谱,原子力显微镜(AFM),透射电子显微镜(TEM)和光致发光研究进行了表征。从AFM,TEM,XRD确定PbS纳米颗粒的尺寸,并且从这些研究中发现,颗粒尺寸约为10-15nm。使用紫外可见光谱和光致发光光谱,在PbS纳米颗粒上观察到了大块材料的“蓝移”。

著录项

  • 来源
    《Materials Chemistry and Physics.》 |2009年第3期|443-447|共5页
  • 作者单位

    Center for Materials Science and Nano Devices, Department of Physics, SRM University, Kattankulathur, Kancheepuram 603203 (D.t.), Tamil Nadu, India;

    Department of Physics, Asan Memorial College of Engineering and Technology, Chengalpattu 603105, Tamil Nadu, India;

    Center for Materials Science and Nano Devices, Department of Physics, SRM University, Kattankulathur, Kancheepuram 603203 (D.t.), Tamil Nadu, India;

    Center for Materials Science and Nano Devices, Department of Physics, SRM University, Kattankulathur, Kancheepuram 603203 (D.t.), Tamil Nadu, India;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    semiconductor; PbS; chemical synthesis; atomic force microscopy (AFM); transmission electron microscopy (TEM); optical properties;

    机译:半导体;铅化学合成原子力显微镜(AFM);透射电子显微镜(TEM);光学性质;

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