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Experimental and statistical analysis on mechanical properties of nano flyash impregnated GFRP composites using central composite design method

机译:中心复合设计法对纳米粉煤灰浸渍GFRP复合材料力学性能的实验和统计分析。

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摘要

Nano flyash impregnated Glass Fibre Reinforced Polymer composites (GFRP) were fabricated using various sizes of filler materials (1000 nm, 264 nm, 198 nm, 94 nm & 68 nm) by handlayup method. Chemical composition and crystallographic structure of the obtained nanoflyash particles were confirmed by energy dispersive X-ray spec-troscopy (EDS) and by X-ray diffraction (XRD) techniques. Field emission scanning electron microscopy (FESEM) was used for characterization of surface morphology of the composite as well as distribution of the nano flyash. Effect of flyash filler size on the fractured surface morphology of the composites is analysed by using the FESEM images. The mechanical properties studied such as tensile strength, compressive strength, flexural strength and hardness of nano flyash impregnated GFRP were significantly enhanced compared with micro flyash impregnated GFRP. Experimental results obtained in this study were statistically analysed using Central Composite Design (CCD) method. A graphical and numerical optimization technique was used to find the predicted value of the responses.
机译:通过手糊法使用各种尺寸的填充材料(1000 nm,264 nm,198 nm,94 nm和68 nm)制造了纳米粉煤灰浸渍的玻璃纤维增​​强聚合物复合材料(GFRP)。通过能量色散X射线能谱(EDS)和X射线衍射(XRD)技术确认了所获得的纳米粉尘颗粒的化学组成和晶体结构。场发射扫描电子显微镜(FESEM)用于表征复合材料的表面形态以及纳米粉煤灰的分布。利用FESEM图像分析了粉煤灰填料尺寸对复合材料断裂表面形态的影响。与微粉煤灰浸渍的GFRP相比,纳米粉煤灰浸渍的GFRP的拉伸强度,抗压强度,弯曲强度和硬度等力学性能得到了显着提高。使用中央复合设计(CCD)方法对本研究中获得的实验结果进行统计分析。使用图形和数字优化技术来找到响应的预测值。

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