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Microstructure and Properties of Spark Plasma Sintering AlN/BN Ceramics

机译:放电等离子烧结AlN / BN陶瓷的组织与性能

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摘要

Aluminum nitride-boron nitride (AlN/BN) composite ceramics were prepared by spark plasma sintering (SPS). The sintering behaviors of AlN/BN composites with 5~15% volume fraction of BN were studied. The influences of BN content, as well as the sintering temperature on the density, microstructure, mechanical strength, thermal conductivity and machinability of the composites were also investigated. The results showed that the full densification of AlN/BN composite ceramics could be realized by SPS technique at the temperature no higher than 1800℃ for 3 minutes. The thermal conductivity of AlN/BN composites is in the range of 66~79W/mK, and AlN/BN composites can be cut or drilled by carbides or even steel tools when BN content is 15% volume fraction. The mechanical strength of AlN/BN composites is about 330MPa and is not remarkably affected by the addition of BN. The improvement of mechanical properties of AlN/BN composite ceramics is due to the fine and homogenous microstructure developed in the SPS process.
机译:通过火花等离子体烧结(SPS)制备了氮化铝-氮化硼(AlN / BN)复合陶瓷。研究了BN体积分数为5〜15%的AlN / BN复合材料的烧结行为。还研究了BN含量以及烧结温度对复合材料的密度,显微组织,机械强度,导热性和可加工性的影响。结果表明,在不超过1800℃的温度下3分钟,采用SPS技术可以实现AlN / BN复合陶瓷的完全致密化。 AlN / BN复合材料的导热系数在66〜79W / mK范围内,当BN含量为15%体积分数时,可用碳化物甚至钢工具切割或钻孔AlN / BN复合材料。 AlN / BN复合材料的机械强度约为330MPa,且不受BN的添加影响。 AlN / BN复合陶瓷的机械性能的改善归因于SPS工艺中形成的精细且均匀的微观结构。

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