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Shape memory response of porous NiTi shape memory alloys fabricated by selective laser melting

机译:选择性激光熔融制备的多孔NiTi形状记忆合金的形状记忆响应

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摘要

Porous NiTi scaffolds display unique bone-like properties including low stiffness and superelastic behavior which makes them promising for biomedical applications. The present article focuses on the techniques to enhance superelasticity of porous NiTi structures. Selective Laser Melting (SLM) method was employed to fabricate the dense and porous (32-58%) NiTi parts. The fabricated samples were subsequently heat-treated (solution annealing + aging at 350 degrees C for 15 min) and their thermo-mechanical properties were determined as functions of temperature and stress. Additionally, the mechanical behaviors of the samples were simulated and compared to the experimental results. It is shown that SLM NiTi with up to 58% porosity can display shape memory effect with full recovery under 100 MPa nominal stress. Dense SLM NiTi could show almost perfect superelasticity with strain recovery of 5.65 after 6% deformation at body temperatures. The strain recoveries were 3.5, 3.6, and 2.7% for samples with porosity levels of 32%, 45%, and 58%, respectively. Furthermore, it was shown that Young's modulus (i.e., stiffness) of NiTi parts can be tuned by adjusting the porosity levels to match the properties of the bones.
机译:多孔NiTi支架显示出独特的骨样特性,包括低刚度和超弹性,这使其在生物医学应用中很有前途。本文重点介绍增强多孔NiTi结构超弹性的技术。选择性激光熔化(SLM)方法用于制造致密和多孔(32-58%)的NiTi零件。随后对制成的样品进行热处理(固溶退火+在350摄氏度下老化15分钟),并根据温度和应力确定其热机械性能。此外,模拟了样品的力学行为并将其与实验结果进行了比较。结果表明,孔隙率高达58%的SLM NiTi可以显示形状记忆效应,并在100 MPa标称应力下完全恢复。致密SLM NiTi在体温6%变形后可显示出近乎完美的超弹性,应变回复率为5.65。孔隙率分别为32%,45%和58%的样品的应变回收率分别为3.5、3.6和2.7%。此外,已经表明,可以通过调节孔隙率水平以匹配骨头的特性来调节NiTi零件的杨氏模量(即,刚度)。

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