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Enhanced microwave absorption properties in cobalt-zinc ferrite based nanocomposites

机译:钴锌铁氧体基纳米复合材料中增强的微波吸收性能

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In an attempt to find a solution to the problem of the traditional spinel ferrite used as the microwave absorber, the Co_(0.6)Zn_(0.4)Fe_2O_4-Paraffin nanocomposites were investigated. Cobalt-zinc ferrite powders, synthesized through PVA sol-gel method, were combined with differing concentrations of Paraffin wax. The nanocomposite samples were characterized employing various experimental techniques including X-Ray Diffraction (XRD), Field Emission Scanning Electron Microscopy (FESEM), Alternating Gradient Force Magnetometer (AGFM), and Vector Network Analyzer (VNA). The saturation magnetization and coercivity were enhanced utilizing appropriate stoichiometry, coordinate agent, and sintering temperature required for the preparation of cobalt-zinc ferrite. The complex permittivity and permeability spectra, and Reflection Loss (RL) of Co_(0.6)Zn_(0.4)Fe_2O_4-Paraffin nanocomposites were measured in the frequency range of 1-18 GHz. The microwave absorption properties of nanocomposites indicated that the absorbing composite containing 20wt% of paraffin manifests the strongest microwave attenuation ability. The composite exhibited the reflection loss less than -10 dB in the whole C-band and 30% of the X-band frequencies.
机译:为了找到解决传统尖晶石型铁氧体用作微波吸收剂的问题的方法,研究了Co_(0.6)Zn_(0.4)Fe_2O_4-石蜡纳米复合材料。通过PVA溶胶凝胶法合成的钴锌铁氧体粉末与不同浓度的石蜡混合。使用各种实验技术对纳米复合材料样品进行表征,包括X射线衍射(XRD),场发射扫描电子显微镜(FESEM),交替梯度力磁力计(AGFM)和矢量网络分析仪(VNA)。利用适当的化学计量比,配位剂和制备钴锌铁氧体所需的烧结温度,可以提高饱和磁化强度和矫顽力。在1-18 GHz的频率范围内测量了Co_(0.6)Zn_(0.4)Fe_2O_4-石蜡纳米复合材料的复介电常数和磁导率谱以及反射损耗(RL)。纳米复合材料的微波吸收特性表明,含20wt%石蜡的吸收复合材料表现出最强的微波衰减能力。该复合材料在整个C波段和X波段频率的30%处的反射损耗均小于-10 dB。

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