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A study of the fluorescent properties of spin-coated sodium salicylate thin films

机译:旋涂水杨酸钠薄膜的荧光特性研究

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Thin films of sodium salicylate were deposited by spin coating from a solution prepared by dissolving sodium salicylate in methanol. The films were characterized by X-ray photoelectron spectroscopy, X-ray diffraction, scanning electron microscopy, UV-visible spectroscopy and spectrofluorometry. The films were crystalline with a strong blue fluorescence peak at an emission wavelength of 419.3 nm. The influence of solution concentration, spin speed and annealing temperature on the fluorescence intensity was studied. Optimum results were obtained with a solution whose concentration was 2.5 M. It was found that lower spin speed resulted in higher fluorescence intensity. Moreover, the fluorescence intensity decreased as the annealing temperature was increased. The durability of the films over a period of 30 days was also investigated, and films annealed at higher temperatures were found to be less degraded with time.
机译:通过将水杨酸钠溶解在甲醇中制备的溶液进行旋涂来沉积水杨酸钠薄膜。通过X射线光电子能谱,X射线衍射,扫描电子显微镜,UV-可见光谱和荧光光谱对膜进行表征。所述膜为晶体,在419.3nm的发射波长处具有强的蓝色荧光峰。研究了溶液浓度,旋转速度和退火温度对荧光强度的影响。使用浓度为2.5 M的溶液可获得最佳结果。发现较低的自旋速度会导致较高的荧光强度。而且,荧光强度随着退火温度的升高而降低。还研究了薄膜在30天内的耐久性,发现在较高温度下退火的薄膜随时间的降解程度较小。

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