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Growth and characterization of novel ferroelectric urea- succinic acid single crystals

机译:新型铁电脲-琥珀酸单晶的生长与表征

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Single crystals of a new ferroelectric material, urea-succinic acid have been grown from aqueous solution by slow evaporation technique up to a dimension of 20 × 10 × 2 mm~3 within a period of 4 weeks. The surface morphology and the structure of the grown crystals were confirmed by single-crystal X-ray diffraction (XRD). The presence of title compound in the crystal lattice has been qualitatively determined by FTIR analysis. The transparency of the grown crystal was confirmed by optical absorption spectrum. The mechanical properties and the thermal stability of the grown crystal were evaluated by Vickers microhardness test and TG/DTA, respectively. The dielectric constant and dielectric loss of the grown crystal was carried out as a function of frequency for different temperatures 413, 433 K, respectively, and the results are discussed.
机译:一种新型的铁电材料脲-琥珀酸的单晶是通过缓慢蒸发技术从水溶液中生长出来的,在4周内达到了20×10×2 mm〜3的尺寸。通过单晶X射线衍射(XRD)证实了生长晶体的表面形态和结构。通过FTIR分析定性地确定了标题化合物在晶格中的存在。通过光吸收光谱确认生长的晶体的透明性。生长晶体的机械性能和热稳定性分别通过维氏显微硬度测试和TG / DTA进行了评估。分别针对不同温度413、433 K进行晶体生长的介电常数和介电损耗随频率的变化,并对结果进行了讨论。

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