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Three-point bending behavior of a Au nanowire studied by in-situ Laue micro-diffraction

机译:原位劳厄微衍射研究金纳米线的三点弯曲行为

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摘要

The elastic and plastic deformation of a gold nanowire tested in a three-point bending configuration using the custom-built scanning force microscope SFINX was studied in situ by Laue micro-diffraction. A new data treatment method based on the integration of diffraction patterns recorded along the deformed nanostructure is introduced visualizing both the movement and shape of the diffraction peaks as a function of the measurement position. Besides bending, torsion is evidenced during the elastic deformation originating from a misalignment of the SFINX-tip of the order of 60 nm with respect to the nanowire center. As demonstrated by post-mortem Laue micro-diffraction maps, the plastic deformation is governed by the storage of geometrically necessary dislocations. Analyzing the shape of the diffraction peaks, the activation of two unexpected slip systems is found which does not coincide with the slip systems with the highest resolved shear stress. These unexpected slip systems are probably related to the dislocation nucleation process at the clamping point, which is influenced by the local curvature. Published by AIP Publishing.
机译:通过劳厄微衍射原位研究了使用定制扫描力显微镜SFINX在三点弯曲配置下测试的金纳米线的弹性和塑性变形。引入了一种新的数据处理方法,该方法基于对沿变形的纳米结构记录的衍射图进行整合,将衍射峰的移动和形状可视化为测量位置的函数。除了弯曲之外,在弹性变形过程中还证明了扭转,这是由于SFINX尖端相对于纳米线中心的未对准程度约为60 nm。如验尸劳厄微衍射图所示,塑性变形由几何必要位错的存储控制。分析衍射峰的形状,发现了两个意外滑动系统的激活,这与具有最高解析剪切应力的滑动系统不一致。这些意外的滑移系统可能与夹紧点处的位错成核过程有关,这受局部曲率的影响。由AIP Publishing发布。

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