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A benign hydrothermal synthesis of nanopencils-like zinc oxide nanoflowers

机译:良性水热法合成纳米铅笔状氧化锌纳米花

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摘要

Synthesis of zinc oxide (ZnO) nanoflowers and nanopencils is normally carried out with the help of structure-directing chemicals and templates. Besides releasing environmentally toxic substances, the use of these chemicals restricts the practical applications of nanostructures. In this paper, we report a typical template-free and environmentally benign synthesis of ZnO nanoflowers with nanopencils-like petals through a facile hydrothermal method. The as-synthesized ZnO nanoflowers were characterized using X-ray diffraction, field emission scanning electron microscopy, tunneling electron microscopy (TEM), high resolution TEM, and energy-dispersive X-ray spectroscopy techniques. The results reveal high quality and impurity-free hexagonal wurtzite phase ZnO nanoflowers of nanopencils-like petals having a length of 100–150nm and a diameter of 45–60nm.
机译:氧化锌(ZnO)纳米花和纳米铅笔的合成通常是在结构导向化学物质和模板的帮助下进行的。除了释放对环境有害的物质外,这些化学物质的使用还限制了纳米结构的实际应用。在本文中,我们报告了一种通过简便的水热方法合成的无模板且对环境无害的ZnO纳米花,其具有类似纳米铅笔状的花瓣。使用X射线衍射,场发射扫描电子显微镜,隧道电子显微镜(TEM),高分辨率TEM和能量色散X射线光谱技术对合成后的ZnO纳米花进行表征。结果表明,纳米铅笔状花瓣的高质量无杂质六角形纤锌矿相ZnO纳米花的长度为100-150nm,直径为45-60nm。

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