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Mean grain size evaluation of tungsten- and boron-carbide composites sintered at various temperatures by ultrasonic methods

机译:用超声方法评估在不同温度下烧结的碳化钨和碳化硼复合材料的平均粒度

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摘要

In this study, the mean grain size of different ceramic-metal composites made from tungsten carbide and boron carbide have been determined with the ultrasonic velocity technique. In addition, the electroless coating method was used to coat the tungsten carbide samples. The prepared samples were sintered at different temperatures ranging from 1200℃ to 1400℃ in an argon atmosphere. Powders were placed in a 30 mm diameter mold and pressed using a hydraulic press at a pressure of 200 bar.rnThe results were compared to the mean grain size obtained from Scanning Electron Microscopy (SEM). This study shows a clear dependence of ultrasonic velocity on grain size in composites of boron carbide and tungsten carbide. Especially the temperature dependence of mean grain size for tungsten carbide composites can be seen very clearly.
机译:在这项研究中,已通过超声速度技术确定了由碳化钨和碳化硼制成的不同陶瓷-金属复合材料的平均晶粒尺寸。另外,使用化学镀方法涂覆碳化钨样品。所制备的样品在氩气氛中在1200℃至1400℃的不同温度下烧结。将粉末放入直径为30 mm的模具中,并使用液压机在200 bar的压力下压制。将结果与从扫描电子显微镜(SEM)获得的平均晶粒尺寸进行比较。这项研究表明超声速度对碳化硼和碳化钨复合材料中晶粒尺寸的明显依赖性。特别是,碳化钨复合材料的平均晶粒尺寸对温度的依赖性非常明显。

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