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Electrical and mechanical behaviour of improved platinum on ceramic bolometers

机译:陶瓷测辐射热计上改进铂的电气和机械性能

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Bolometers using Au meanders on a mica substrate under irradiation suffered severe degradation before 0.01 dpa. Therefore this work was undertaken to examine alternative more radiation resistant bolometer versions. Basic prototypes from CIEMAT with sputtered Pt meander sensors on Al_2O_3 and A1N ceramic substrates were tested during electron and neutron irradiation at CIEMAT and SCK/CEN Mol. Results up to 0.01 dpa showed acceptable behaviour of both substrates and better radiation resistance response of Pt compared with Au. However the electrical connection between terminals and meander was identified as a weak point of the design. In addition the electrical response of the sputtered metal films was observed to degrade at high temperatures ( > 900 ℃) as a consequence of the discontinuity of the thin metal film and the formation of Pt islands.rnHere we report on an improved prototype, with reduced meander area, enhanced Pt film quality and adhesion, and better electrical connections. The improved bonding and hence stability of the meander was obtained by sputtering and thermally evaporating a Pt sensor on to polished surfaces of A1N and Al_2O_3 substrates. The thermal stability of the sputtered Pt deposit has also been followed using ESEM during in situ sample heating. After vacuum annealing at 400 ℃, these new prototypes were electrically characterized.
机译:在辐照下,在云母基底上使用金曲折的Bolometer在0.01 dpa之前遭受严重降解。因此,这项工作是为了研究替代的更耐辐射的辐射热测量计。在CIEMAT和SCK / CEN Mol的电子和中子辐照过程中,测试了CIEMAT的基本原型,该原型在Al_2O_3和AlN陶瓷衬底上具有溅射的Pt曲折传感器。高达0.01 dpa的结果表明,与Au相比,两种基材的性能均可接受,Pt的抗辐射性能更好。但是,端子和曲折之间的电连接被认为是设计的薄弱点。此外,由于金属薄膜的不连续性和Pt岛的形成,在高温(> 900℃)下观察到溅射金属膜的电响应会降低。弯曲的区域,增强的Pt膜质量和附着力以及更好的电气连接。通过将Pt传感器溅射并热蒸发到AlN和Al_2O_3基板的抛光表面上,可以提高曲折性,从而提高曲折的稳定性。在原位样品加热过程中,还使用ESEM跟踪了溅射的Pt沉积物的热稳定性。经过400℃的真空退火后,对这些新原型进行了电学表征。

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