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SiC-based sandwich material for Flow Channel Inserts in DCLL blankets: Manufacturing, characterization, corrosion tests

机译:用于DCLL毯中流道嵌件的SiC基三明治材料:制造,表征,腐蚀测试

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Flow Channel Inserts (FCIs) are key elements in a DCLL blanket concept for DEMO, since they provide the required thermal insulation between the He cooled structural steel and the hot liquid PbLi flowing at approximate to 700 degrees C, and the necessary electrical insulation to minimize MHD effects. In this work a SiC-based sandwich material is proposed for FCIs, consisting of a porous SiC core covered by a dense CVD-SiC layer. A method to produce the porous SiC core is presented, based on combining a starting mixture of SiC powder with a spherical carbonaceous sacrificial phase, which is removed after sintering by oxidation, in such a way that a microstructure of spherical pores is achieved. Following this technique, a porous SiC material with low thermal and electrical conductivities, but enough mechanical strength was produced. Samples were covered by a 200 mu m thick CVD-SiC coating to form a SiC-sandwich material. Finally, corrosion tests under static PbLi were performed, showing that such a dense layer offers a reliable protection against static PbLi corrosion. (C) 2017 Elsevier B.V. All rights reserved.
机译:流道嵌件(FCI)是用于DEMO的DCLL覆盖层概念中的关键元素,因为它们在He冷却的结构钢和流动到大约700摄氏度的热液体PbLi之间提供了所需的绝热,并提供了必要的电气绝缘以最大程度地减少MHD效果。在这项工作中,提出了一种用于FCI的基于SiC的夹层材料,该材料由被致密CVD-SiC层覆盖的多孔SiC芯组成。提出了一种制造多孔SiC核的方法,其基于将SiC粉末的起始混合物与球形碳质牺牲相混合,该碳质牺牲相在通过氧化烧结之后被去除,从而获得球形孔的微观结构。按照这种技术,可以生产出具有低导热性和导电性但具有足够机械强度的多孔SiC材料。用200μm厚的CVD-SiC涂层覆盖样品以形成SiC夹心材料。最后,进行了在静态PbLi下的腐蚀测试,结果表明,这种致密层可提供可靠的防静电PbLi腐蚀保护。 (C)2017 Elsevier B.V.保留所有权利。

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