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A rheological characterization of semi-solid dairy systems

机译:半固态乳制品系统的流变学表征

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Dispersions of cross-linked starch in full fat milk, taken as models of custard model systems, have been characterized by different rheological means: viscoelastic measurements, classical flow measurements and 'vane' rheometry. From viscosity measurements, the flow behaviour was described within the shear rate range 0.01-100 s~(-1). The flow curves were fitted using the Herschell-Bulkley equation over the shear rate range 0.1-100 s~(-1) while a deviation was found towards the low shear rate range, making the determination of the yield stress non realistic. Instead, measurements with the 'vane' device in low shear conditions provided a way to estimate the yield stress, at rest and after shearing, but the entire flow curve was not described. From the viscoelastic measurements at low strain amplitude, the mechanical spectra were obtained. Linearity tests beyond the linearity limits provided the critical stress corresponding to the G′-G″ cross-over. The parameters obtained from these different rheological methods are discussed.
机译:作为乳蛋糕模型系统的模型,全脂牛奶中交联淀粉的分散体具有不同的流变学特性:粘弹性测量,经典流量测量和“叶片”流变法。通过粘度测量,在0.01-100 s〜(-1)的剪切速率范围内描述了流动行为。使用Herschell-Bulkley方程在0.1-100 s〜(-1)的剪切速率范围内拟合流动曲线,同时发现在低剪切速率范围内存在偏差,这使得确定屈服应力变得不现实。取而代之的是,在低剪切条件下用“叶片”装置进行的测量提供了一种估算在静止和剪切后的屈服应力的方法,但并未描述整个流动曲线。从低应变幅度下的粘弹性测量中,获得了机械光谱。超出线性极限的线性测试提供了与G'-G''交叉对应的临界应力。讨论了从这些不同的流变方法获得的参数。

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