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Development and optimisation of a non conventional extraction process of natural dye from olive solid waste using response surface methodology (RSM)

机译:使用响应表面方法(RSM)开发和优化非常规提取橄榄固体废物中天然染料的工艺

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摘要

Dyes obtained from different natural sources have emerged as an important alternative to synthetic dyes. In this study, optimisation of natural colorant non-conventional extraction technique from olive waste was investigated using response surface methodology. The combined effects of extraction conditions on total phenolic content (TPC) and relative color strength (K/S) were studied using a three-level three-factor Box-Behnken design. The optimum conditions for dye extraction were found to be 0.14 mol/L, 62.11 min, 71.23 ℃ and 4.5 g for sodium hydroxide concentration, extraction time, temperature, and mass of the waste, respectively. The efficiency of extraction under these optimum conditions was found to be 1133.86 mg/L of pheno-lics and relative GUELour strength (K/S) equal to 23.22. Further, Fourier Transform Infrared Spectroscopy was used to identify the major chemical groups in the extracted dye.
机译:从不同天然来源获得的染料已成为合成染料的重要替代品。在这项研究中,使用响应面方法研究了从橄榄色废料中天然色素非常规提取技术的优化。使用三级三因素Box-Behnken设计研究了萃取条件对总酚含量(TPC)和相对色强度(K / S)的综合影响。最佳的提取条件为氢氧化钠浓度,提取时间,温度和废物质量分别为0.14 mol / L,62.11 min,71.23℃和4.5 g。发现在这些最佳条件下的萃取效率为1133.86 mg / L苯酚,相对GUELour强度(K / S)等于23.22。此外,使用傅立叶变换红外光谱法鉴定提取的染料中的主要化学基团。

著录项

  • 来源
    《Food Chemistry》 |2014年第15期|345-352|共8页
  • 作者单位

    Research Unit of Applied Chemistry and Environment, Faculty of Sciences of Monastir, 5000 Monastir, Tunisia;

    Research Unit of Applied Chemistry and Environment, Faculty of Sciences of Monastir, 5000 Monastir, Tunisia;

    Research Unit of Applied Chemistry and Environment, Faculty of Sciences of Monastir, 5000 Monastir, Tunisia;

    Research Unit of Applied Chemistry and Environment, Faculty of Sciences of Monastir, 5000 Monastir, Tunisia;

    Research Unit of Applied Chemistry and Environment, Faculty of Sciences of Monastir, 5000 Monastir, Tunisia;

  • 收录信息 美国《科学引文索引》(SCI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    Olive waste; Extraction; Response surface methodology; Optimisation;

    机译:橄榄废料;萃取;响应面方法;优化;

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