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Eleven phthalate esters and di(2-ethylhexyl) adipate in one- week duplicate diet samples obtained from hospitals and their estimated daily intake

机译:从医院获得的一星期重复饮食样本中的十一种邻苯二甲酸酯和己二酸二(2-乙基己基)酯及其估计的每日摄入量

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摘要

Plasticizers in duplicate diet samples obtained over 1 week were analysed in order to estimate daily intake. The phthalate esters we as follows: diethyl, dipropyl, Dibutyl, dipentyl, dihexyl, butylbenzyl, dicyclohexyl, Di(2-ethylhexyl), dioxtyl, diisooctyl (mixture of iso- Mers) and diisononyl (mixture). Di(2-ehtylhexyl) Adipate was also determined. Homogenized samples of Composite meals were extracted with acetonitrile, lipids Were removed by extraction into n-hexane and the Acetonitrile layer was cleaned using Florisil~R and Bondesil PSA~R dual layer column.
机译:分析超过1周的双份饮食样品中的增塑剂,以估计每日摄入量。邻苯二甲酸酯如下:二乙基,二丙基,二丁基,二戊基,二己基,丁基苄基,二环己基,二(2-乙基己基),二氧己基,二异辛基(异丁烯的混合物)和二异壬基(混合物)。还确定了己二酸二(2-乙基己基)酯。用乙腈提取均质的复合粉样品,通过萃取到正己烷中除去脂质,并使用Florisil®R和BondesilPSA®R双层色谱柱清洁乙腈层。

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