EPA REGULATIONS ON NATIONAL EMISSION STANDARDS FOR HAZARDOUS AIR POLLUTANTS FOR SOURCE CATEGORIES—APPENDICES

摘要

Method 301-Field Validation of Pollutant Measurement Methods From Various Waste MediaSec.Using Method 3011.0 What is the purpose of Method 301?2.0 What approval must I have to use Method 301?3.0 What does Method 301 include?4.0 How do I perform Method 301?Reference Materials5.0 What reference materials must I use?Sampling Procedures6.0 What sampling procedures must I use?7.0 How do I ensure sample stability?Determination of Bias and Precision8.0 What are the requirements for bias?9.0 What are the requirements for precision?10.0 What calculations must I perform for isotopic spiking?11.0 What calculations must I perform for comparison with a validated method?12.0 What calculations must I perform for analyte spiking?13.0 How do I conduct tests at similar sources?Optional Requirements14.0 How do I use and conduct ruggedness testing?15.0 How do I determine the Limit of Detection for the candidate test method?Other Requirements and Information16.0 How do I apply for approval to use a candidate test method?17.0 How do I request a waiver?18.0 Where can I rind additional information?19.0 Tables.Using Method 3011.0 What is the purpose of Method 301?Method 301 provides a set of procedures for the owner or operator of an affected source to validate a candidate test method as an alternative to a required test method basedon established precision and bias criteria. These validation procedures are applicable under 40 CFR part 63 or 65 when a test method is proposed as an alternative test method to meet an applicable requirement or in the absence of a validated method. Additionally, the validation procedures of Method 301 are appropriate for demonstration of the suitability of alternative test methods under 40 CFR parts 59. 60, and 61. If. under 40 CFR part 63 or 60. you choose to propose a validation method other than Method 301. you must submit and obtain the Administrator's approval for the candidate validation method.