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Preparation of modified magnesium hydroxide and its application in PA66

机译:改性氢氧化镁的制备及其在PA66中的应用

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In the present study,the modified magnesium hydroxide was prepared by precipitation method using Mg(NO_(3)), NaOH, and silane coupling 702 modifier as raw materials. The optimal reaction conditions were obtained as follows: sodium hydroxide was added to magnesium nitrate solution by dropping, the dropping speed of sodium hydroxide was 2ml/min, the reaction temperature was 60°C, and the ratio of modifier dosage to total solution volume was 7/100(g/ml). The oil absorption value and XRD were used to characterize the modified Mg(OH)_(2). In the application, the modified magnesium hydroxide was mixed with pentaerythritol octahydrogen tetraphosphate(PEPA) and applied to nylon 66(PA66).The flame retardancy and mechanical properties of the nylon 66(PA66)composite were studied.
机译:在本研究中,通过使用Mg(NO_(3)),NaOH和硅烷偶联702改性剂作为原料,通过沉淀法制备改性氢氧化镁。如下取得最佳反应条件:通过滴加将氢氧化钠加入硝酸镁溶液中,氢氧化钠的滴速为2ml / min,反应温度为60℃,改性剂剂量与总溶液体积的比例为总溶液7/100(g / ml)。吸油值和XRD用于表征改性的Mg(OH)_(2)。在施用中,将改性的氢氧化镁与季戊四醇八磷酸(Pepa)混合并施加到尼龙66(PA66)上。研究了尼龙66(PA66)复合材料的阻燃性和力学性能。

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