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Turbidimetric Measurement for On-line Monitoring of SiO2 Particles

机译:SiO 2 颗粒在线监测的浊度测量

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In this work, the fundamental study of on-line monitoring of SiO2 particles in the size range of 40 nm to 725 nm was carried out using turbidimetry. The size of particle was measured using a field emission scanning electron microscope (FE-SEM). The factors affecting on the turbidity were discussed, for example, wavelength, size, and concentration. In order to observe the dependence of turbidity on the wavelength, a turbidimetric system equipped with charged coupled detector (CCD) was built. The shape of the transmitted peak was changed and the peak maximum was shifted to the red when the concentration of particle was increased. This result indicates that the turbidity is related to the wavelength, which corresponds to the characteristic of the Mie extinction coefficient, Q, that is a function of not only particle diameter and refractive index but also wavelength. It is clear that a linear calibration curve for each particle in different size can be obtained at an optimized wavelength.
机译:在这项工作中,使用比浊法对40 nm至725 nm尺寸范围内的SiO2颗粒进行在线监测的基础研究。使用场发射扫描电子显微镜(FE-SEM)测量颗粒的尺寸。讨论了影响浊度的因素,例如波长,大小和浓度。为了观察浊度对波长的依赖性,建立了配备有电荷耦合检测器(CCD)的比浊系统。当增加颗粒浓度时,透射峰的形状发生变化,并且峰最大值变为红色。该结果表明浊度与波长有关,这与米氏消光系数Q的特性相对应,该特性不仅是粒径和折射率的函数,而且是波长的函数。显然,可以在优化的波长下获得不同尺寸的每个颗粒的线性校准曲线。

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