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Determination of Nickel by EDTA Titration

机译:EDTA滴定法测定镍

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The nickel has been separated and precipitated with dimethylglyoxime in the usual manner and dissolved the precipitates with hydrochloric acid. To the nickel solution, 0.2g of Murexide as an indicator and 5 ml of 20 percent tri-ethanol amine solution were added and titrated with a standard solution of EDTA. At the end point the color changes from yellow to deep purple. In this paper, the purpose is that conditions for titration and for separation from the interfering substances were investigated and a suitable procedure was found and applied on the determination of nickel in Korean nickel ores.
机译:以通常的方式分离镍并用二甲基乙二肟沉淀,并用盐酸溶解沉淀。向镍溶液中加入0.2g的Murexide指示剂和5ml的20%三乙醇胺溶液,并用EDTA标准溶液滴定。最后,颜色从黄色变为深紫色。本文旨在研究滴定和与干扰物分离的条件,并找到合适的程序并将其应用于韩国镍矿中镍的测定。

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