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Preparation of alumina-iron oxide compounds by coprecipitation and gel evaporation methods and their characterization

机译:共沉淀和凝胶蒸发法制备氧化铝-氧化铁化合物及其表征

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Fe2O3-Al2O3??compounds were synthesized by coprecipitation(CP) and gel evaporation (GE) method with different Fe/Al compositions andcalcined at high temperatures (300oC-1000oC). Thecrystalline phases in the samples were determined by XRD, the latticeparameters of the resulting crystalline phases were calculated by aleast-square method. The properties were also characterized by magnetizationmeasurements. The formation of crystalline phases (e.g., maghemite, hematite),transformation temperature, magnetic properties of iron oxide were all affectedby the component ratio and thermal treatment.
机译:通过共沉淀(CP)和凝胶蒸发(GE)的方法,用不同的Fe / Al组成合成了Fe2O3-Al2O3β3化合物,并在高温(300oC-1000oC)下煅烧。用X射线衍射仪测定样品中的晶相,并采用最小二乘方法计算所得晶相的晶格参数。还通过磁化测量来表征性能。组分比和热处理均影响结晶相(例如磁赤铁矿,赤铁矿)的形成,相变温度,氧化铁的磁性能。

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