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Exploration of Mechanical and Thermal Properties of CTAB-Modified MoS2/LLDPE Composites Prepared by Melt Mixing

机译:熔体混合法制备CTAB改性的MoS2 / LLDPE复合材料的力学和热性能

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Molybdenum disulfide (MoS2) was functionalized by cetyltrimethylammonium bromide (CTAB) through a one-pot hydrothermal technique, and subsequently, linear low-density polyethylene (LLDPE) composites were prepared. The attachment of alkyl chains of CTAB onto the MoS2 surface was confirmed by Fourier transform infrared spectroscopy (FTIR). The enhanced mechanical properties of the composites relative to neat LLDPE revealed good compatibility between MoS2 and LLDPE. The improvement in thermomechanical properties further substantiated good interaction between MoS2 and LLDPE. The thermal stability of the prepared composites showed a small decrease in onset degradation temperature. Nevertheless, the char residue formation was found to be promoted in the presence of MoS2.
机译:通过一锅水热技术,通过十六烷基三甲基溴化铵(CTAB)对二硫化钼(MoS2)进行功能化,然后制备线性低密度聚乙烯(LLDPE)复合材料。通过傅立叶变换红外光谱法(FTIR)证实了CTAB的烷基链在MoS 2表面上的附着。相对于纯LLDPE,复合材料机械性能增强,表明MoS2和LLDPE之间具有良好的相容性。热力学性能的改善进一步证实了MoS2和LLDPE之间的良好相互作用。制备的复合材料的热稳定性显示开始降解温度略有降低。然而,发现在MoS 2存在下促进了残炭的形成。

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