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首页> 外文期刊>Journal of Advanced Ceramics >Evaluating high temperature elastic modulus of ceramic coatings by relative method
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Evaluating high temperature elastic modulus of ceramic coatings by relative method

机译:通过相关方法评估陶瓷涂层的高温弹性模量

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The accurate evaluation of the elastic modulus of ceramic coatings at high temperature (HT) is of high significance for industrial application, yet it is not easy to get the practical modulus at HT due to the difficulty of the deformation measurement and coating separation from the composite samples. This work presented a simple approach in which relative method was used twice to solve this problem indirectly. Given a single-face or double-face coated beam sample, the relative method was firstly used to determine the real mid-span deflection of the three-point bending piece at HT, and secondly to derive the analytical relation among the HT moduli of the coating, the coated and uncoated samples. Thus the HT modulus of the coatings on beam samples is determined uniquely via the measured HT moduli of the samples with and without coatings. For a ring sample (from tube with outer-side, inner-side, and double-side coating), the relative method was used firstly to determine the real compression deformation of a split ring sample at HT, secondly to derive the relationship among the slope of load-deformation curve of the coated ring, the HT modulus of the coating and substrate. Thus, the HT modulus of ceramic coatings can be evaluated by the substrate modulus and the load-deformation data of coated rings. Mathematic expressions of those calculations were derived for the beam and ring samples. CVD-SiC coatings on graphite substrate were selected as the testing samples, of which the measured modulus ranging from room temperature to 2100 °C demonstrated the validity and convenience of the relative method.
机译:陶瓷涂层在高温(HT)下的弹性模量的准确评估对工业应用具有重要意义,但是由于变形测量和涂层与复合材料之间的分离困难,在高温下很难获得实用的模量样品。这项工作提出了一种简单的方法,其中两次使用相对方法间接解决此问题。对于单面或双面镀膜梁样品,首先采用相对方法确定三点弯曲件在HT处的真实中跨挠度,其次推导三点弯曲件在HT模量之间的解析关系。涂层,涂层样品和未涂层样品。因此,光束样品上涂层的HT模量是通过测量有无涂层的样品的HT模量唯一确定的。对于环形样品(来自具有外侧,内侧和双面涂层的管),首先使用相对方法确定开口环样品在HT处的实际压缩变形,其次推导两者之间的关系。涂层环的载荷-变形曲线的斜率,涂层和基材的HT模量。因此,可以通过基材模量和涂层环的载荷变形数据评估陶瓷涂层的HT模量。这些计算的数学表达式是针对梁和环样本得出的。选择石墨基体上的CVD-SiC涂层作为测试样品,在室温至2100°C范围内测得的模量证明了该方法的有效性和便利性。

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