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Thermal behavior of semiconductor bismuth iodate [Bi(IO3)3] crystals grown by silica gel

机译:硅胶生长的碘酸铋半导体[Bi(IO3)3]晶体的热行为

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The Bismuth Iodate [Bi(IO3)3] crystals have been grown in Sodium meta silicate gel using the Single diffusion method at room temperature. The grown crystals were characterized by thermo analytical techniques (TGA, DTA, DTG and DSC) to estimate its electrical properties like conductivity. X-ray powder diffraction (XRD), By powder X-ray diffraction analysis the crystal structure is confirmed to be Monoclinic, having lattice parameters a = 6.09 A° , b = 16.68 A° , and c = 5.58 A° . Thermal study reveals that Bismuth Iodate crystal is Octa-hydrous. TGA, DTA, DTG and DSC analysis shows a remarkable thermal stability.
机译:碘化铋[Bi(IO3)3]晶体已在室温下使用单扩散法在偏硅酸钠凝胶中生长。通过热分析技术(TGA,DTA,DTG和DSC)对生长的晶体进行了表征,以估算其电性能,如电导率。 X射线粉末衍射(XRD),通过粉末X射线衍射分析,确认晶体结构为单斜晶,其晶格参数为a = 6.09A°,b = 16.68A°和c = 5.58A°。热学研究表明碘酸铋晶体是八水合的。 TGA,DTA,DTG和DSC分析显示出显着的热稳定性。

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