Synthesis and Crystal Structure of a Dinuclear Manganese(III) Complex of 1-[(2-Hydroxymethylphenyl)iminomethyl]-2-naphthol

Ryuji MATSUNAGA; Yasunori YAMADA; Masayuki KOIKAWA; Tadashi TOKII

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Synthesis and Crystal Structure of a Dinuclear Manganese(III) Complex of 1-[(2-Hydroxymethylphenyl)iminomethyl]-2-naphthol

机译：1-[（2-羟基甲基苯基）亚氨基甲基] -2-萘酚的双核锰（III）配合物的合成和晶体结构

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A dinuclear manganese(III) complex, [Mn(L1-Bz)(na)]₂ [H₂L1-Bz = 1-[(2-hydroxymethylphenyl)iminomethyl]-2-naphthol, Hna = o-hydroxynaphthaldehyde], was synthesized and characterized by single-crystal X-ray analysis. The compound crystallizes in a monoclinic system, spaces group P2₁/n and Z = 4 with cell parameters a = 10.080(4)Å, b = 23.642(8)Å, c = 10.368(4)Å, β = 115.142(5)°, V = 2236.6(14)Å3. The dinuclear structure is formed by two μ-hydoroxo bridges with a Mn…Mn separation of 3.1648(14)Å.

机译：双核锰（III）配合物，[Mn（L1-Bz）（na）] _{2 [H _{2 L1-Bz = 1-[（（2-羟甲基苯基）亚氨基甲基]合成并通过单晶X射线分析表征] -2-萘酚，Hna ＝ -羟基萘醛]。该化合物在单斜晶系系统中结晶，空间参数 P 2 _{1 / n 和 Z = 4，且具有细胞参数 a = 10.080（4）Å， b = 23.642（8）Å， c = 10.368（4）Å，β< / i> = 115.142（5）°， V = 2236.6（14）Å 3 。双核结构由两个μ-hydoroxo桥形成，Mn…Mn间距为3.1648（14）Å。}}}

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《X-ray Structure Analysis Online》 |2010年第4期|共2页
作者
Ryuji MATSUNAGA; Yasunori YAMADA; Masayuki KOIKAWA; Tadashi TOKII;
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Synthesis and Crystal Structure of a Dinuclear Manganese(III) Complex of 1-[(2-Hydroxymethylphenyl)iminomethyl]-2-naphthol

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