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首页> 外文期刊>Transactions of the Japan Society for Computational Engineering and Science >Compact Sub Micro-resolution X-ray Microscope Based on Carbon Nanotube FE-SEM
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Compact Sub Micro-resolution X-ray Microscope Based on Carbon Nanotube FE-SEM

机译:基于碳纳米管FE-SEM的紧凑型亚显微X射线显微镜

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Generally, nano-resolution X-ray imaging has been achieved using synchrotron radiation facility. The spatial resolution (below 100 nm) achieved with a Fresnel zone plate for focusing the X-ray in SPring-8 lately. We have developed a compact composite of field emission-scanning electron microscope (FE-SEM) with a single isolated multi-walled carbon nanotube (CNT) electron source in our previous study. The spatial resolution of SEM image was estimated as ≃ 10 nm. This result indicates that the electron source we developed is suitable for a point-like X-ray source. We developed two kinds of X-ray microscope; projection-type X-ray microscope (PXM) and transmission-type X-ray microscope (TXM) in this study. The X-ray microscope based on the CNT-FE-SEM was constructed with a metal target for the X-ray source. Developing our X-ray microscope has been miniaturized to a compact size so that it can be placed on a desk. Moreover, the spatial resolution of 400 nm achieved the theoretical resolution limit. Because there is resolution limit by the acceleration voltage of 17 kV for the focused electron beam spot, the spatial resolution is an order of the electron penetration depth. The present study shows a potential that the CNT-based X-ray microscope would be applied to various field studies including the scene of an archaeological site excavation and future planet search.
机译:通常,已经使用同步加速器辐射设施实现了纳米分辨率的X射线成像。最近使用菲涅耳波带片将X射线聚焦在SPring-8中实现了空间分辨率(低于100 nm)。在先前的研究中,我们已经开发了一种紧凑的场发射扫描电子显微镜(FE-SEM)复合物,其中包含一个孤立的多壁碳纳米管(CNT)电子源。 SEM图像的空间分辨率估计约为10 nm。该结果表明,我们开发的电子源适用于点状X射线源。我们开发了两种X射线显微镜;投影型X射线显微镜(PXM)和透射型X射线显微镜(TXM)。使用金属靶作为X射线源,构建了基于CNT-FE-SEM的X射线显微镜。我们将X射线显微镜的开发规模缩小到了紧凑的尺寸,因此可以将其放在桌子上。此外,400 nm的空间分辨率达到了理论分辨率极限。由于聚焦电子束点受到17 kV加速电压的分辨率限制,因此空间分辨率是电子穿透深度的数量级。本研究表明,基于CNT的X射线显微镜可能会应用于各种现场研究,包括考古现场发掘现场和未来的行星搜索。

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