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A new procedure for a zeolite synthesis from natural clays

机译:由天然粘土合成沸石的新方法

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This work proposes the synthesis of zeolite A by IZA standard proceedures starting from a natural clay. The clay was used in its natural form and after calcination at 900?oC. The resulting materials were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and porosity analysis by nitrogen adsorption. Results showed low surface area for Na-A zeolite in sodium form, but a higher one in CaA based on the nitrogen accessibility. The presence of cubic crystals for the A phase was observed in the SEM micrographies. The new procedure starting from natural clay favors the formation of sodalite while that using the calcinated clay gives A.
机译:这项工作提出了通过IZA标准程序从天然粘土开始合成沸石A的方法。该粘土以其天然形式并在900°C下煅烧后使用。通过X射线衍射(XRD),扫描电子显微镜(SEM)和通过氮吸附的孔隙率分析来表征所得材料。结果表明,钠形式的Na-A沸石表面积较小,但基于氮的可及性,CaA表面积较大。在SEM显微图中观察到A相的立方晶体的存在。从天然粘土开始的新方法有利于形成方钠石,而使用煅烧粘土则得到A。

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