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A study of grain and particle sizes of 40%Ni-Fe, 50%Ni-Fe and 75%Ni-Fe nanopowder prepared by mechanical alloying

机译:机械合金化制备40%Ni-Fe,50%Ni-Fe和75%Ni-Fe纳米粉的晶粒和粒径的研究

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Mechanical alloying through high energy ball milling was used to produce Ni-Fe alloy powders starting from elemental Ni and Fe powders of average particle size 80 and 25μm respectively. High Energy Planetary ball milling at room temperature was performed for various time durations ranging between 2 to 100hours. X-ray Diffraction (XRD) and Particle Size Analyzer were used for characterization of powders. Comparing the three alloys when the percentage of nickel increases the rate of reduction of grain and particle size decreases. During mechanical alloying while the grain size changes the particle size almost remain constant or the particle size changes the grain size almost remain constant. This may be due to the energy consumption either changes in grain size or particle size during mechanical alloying.
机译:通过高能球磨进行机械合金化,从平均粒径分别为80和25μm的元素Ni和Fe粉末开始生产Ni-Fe合金粉末。在室温下进行2到100小时不等的高能行星式球磨。 X射线衍射(XRD)和粒度分析仪用于表征粉末。比较三种合金,当镍的百分比增加时,晶粒的减少率减小,而粒度减小。在机械合金化期间,当晶粒尺寸改变时,晶粒尺寸几乎保持恒定,或者晶粒尺寸改变时晶粒尺寸几乎保持恒定。这可能是由于机械合金化过程中晶粒尺寸或颗粒尺寸的能耗降低所致。

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