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Alkaloids from Mongolian species of Peganum multisectum (Maxim) Bobrov

机译:蒙古Peganum multisectum(Maxim)Bobrov的蒙古生物碱

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Alkaloids of the aerial parts of P. multisectum (Maxim) Bobrov (Zygophyllaceae) growing in Mongolia have been studied by capillary Gas Chromatography-Mass Spectrometry (GC-MS) and Column Chromatography (CC). Four compounds comprising of 2-methylquinoline ( 1 ), 9-amino-2, 3,5,6,7,8-hexahydro-1H-cyclopenta [b] quinoline ( 2 ), vasicinone ( 3 ) and harmine ( 4 ) have been determined by GC-MS, while harmine ( 4 ), peganine ( 5 ), deoxypeganine ( 6 ), deoxyvasicinone ( 7 ) and harmane ( 8 ) were isolated as pure compounds by the CC. The structures of the five alkaloids 4 , 5 , 6 , 7 and 8 were elucidated by the MS and 1 H and 13 C NMR analysis. The alkaloids 1 , 2 and 8 were identified for the first time from this species. Mongolian Journal of Chemistry 16 (42), 2015, 48-53.
机译:通过毛细管气相色谱-质谱法(GC-MS)和柱色谱法(CC)研究了蒙古生长的多假单胞菌(Maxim)Bobrov(Zygophyllaceae)地上部分的生物碱。由2-甲基喹啉(1),9-氨基-2、3,5,6,7,8-六氢-1H-环戊[b]喹啉(2),vasicinone(3)和harmine(4)组成的四种化合物具有通过GC-MS测定,而CC将香豆素(4),豌豆碱(5),脱氧peganine(6),脱氧vasicinone(7)和harmane(8)分离为纯净化合物。通过MS和1 H和13 C NMR分析阐明了五个生物碱4、5、6、7和8的结构。首次从该物种中鉴定出生物碱1、2和8。蒙古化学学报16(42),2015,48-53。

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